RT info:eu-repo/semantics/article T1 Comparison of Activation Methods for 3D-Printed Electrodes for Microbial Electrochemical Technologies A1 Alonso García, Raúl Marcos A1 San Martin Bécares, María Isabel A1 Morán Palao, Antonio A1 Escapa González, Adrián A2 Ingenieria Electrica K1 Electrotecnia K1 Ingeniería química K1 Microbial electrochemical technologies K1 Bioanode K1 Exoelectrogen K1 Graphene K1 3D printing K1 2302.20 Química Microbiológica K1 3313.24 Maquinaria de Impresión y Reproducción AB [EN] Three-dimensional printing could provide flexibility in the design of a new generation of electrodes to be used in microbial electrochemical technologies (MET). In this work, we demonstrate the feasibility of using polylactic acid (PLA)/graphene—a common 3D-printing material—to build custom bioelectrodes. We also show that a suitable activation procedure is crucial to achieve an acceptable electrochemical performance (plain PLA/graphene bioanodes produce negligible amounts of current). Activation with acetone and dimethylformamide resulted in current densities similar to those typically observed in bioanodes built with more conventional materials (about 5 Am−2). In addition, the electrodes thus activated favored the proliferation of electroactive bacteria. PB MDPI LK https://hdl.handle.net/10612/20271 UL https://hdl.handle.net/10612/20271 NO Alonso, R. M., Martín Bécares, I. S., Morán, A., & Escapa, A. (2022). Comparison of activation methods for 3D-printed electrodes for microbial electrochemical technologies. Applied Sciences (Switzerland), 12(1). https://doi.org/10.3390/APP12010275 NO Supplementary Materials: The following supporting information can be downloaded at: https://www.mdpi.com/article/10.3390/app12010275/s1, Figure S1. Current density profiles of two successive cycles at the end of a 60 days period that allowed for the development of a stable biofilm; Table S1: Fitted parameters to EC 1 (DMF and acetone electrodes); Table S2: Fitted parameters to EC 2 (control and electrochemical-treated electrodes); Figure S2. Equivalent circuits for abiotic electrode essays’ modellization.1) DMF and acetone 2) Control and electrochemical treatment. DS BULERIA. Repositorio Institucional de la Universidad de León RD 26-jun-2024